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Part II: Run Time Adjustment

After the standard agreement criteria have been met, determine an appropriate run time (usually 60 minutes) by injecting a sample. Examine the chromatogram and, if necessary, adjust the run time so that all of the peaks due to Cremophor El components are eluted prior to the next injection. If the Cremophor El - related peaks are not resolved from the BMS - 181339 - 01 peak, replace the column. If it is necessary to be certain which peaks are placebo - related, then a placebo working solution may be prepared as per the working sample solution directions and injected.